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河北祥鹄科学仪器有限公司

200A Microwave Extraction Process and Antibacterial Activity of Mountain Blue Red Pigment

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[Abstract]:
NoteTheresearcher,fromtheDepartmentofChemistryandBioengineeringofGuangxiNormalUniversity,completedthepaperonthemicrowaveextractionprocessandantibacterialactivityofthemountainblueredpigment,publishedin
Note

The researcher, from the Department of Chemistry and Bioengineering of Guangxi Normal University, completed the paper on the microwave extraction process and antibacterial activity of the mountain blue red pigment, published in the important journal .

Abstract

Taking plant mountain blue as raw material, microwave solvent assisted extraction of red pigment. The extraction process was optimized by single factor experiment and orthogonal experiment, and the red pigment fraction was preliminarily purified by column chromatography. The results showed that the microwave power was 300 W, the ratio of material to liquid was 1:40 (m /V), the extraction temperature was 60 °C, and the extraction time was 9 min. The optimum conditions for microwave extraction of sapphire red pigment were obtained. The extraction rate was 0.323%. The mulberry red pigment has an inhibitory effect on Escherichia coli, Bacillus subtilis, Candida albicans and Staphylococcus aureus, and the minimum inhibitory concentrations are 500, 400, 700, 500 mg L -1 , respectively.

Details

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Conclusion

The aqueous extract of the mountain blue plant was extracted by microwave extraction, and the red color part was separated and separated by column chromatography for bacteriostatic experiments. Microwave extraction time, solid-liquid ratio, extraction temperature and microwave power have an effect on the extraction efficiency. The degree of influence is extraction time > extraction temperature > material-to-liquid ratio > microwave power, microwave power 300 W, material-to-liquid ratio 1: 40 (m / V), extraction temperature 60 °C, extraction time 9 min is the best extraction condition, the extraction rate of sapphire red pigment reaches 0.323%, and has good stability. Bacteriostatic experiments showed that mulberry red pigment showed antibacterial effect against Escherichia coli, Bacillus subtilis, Candida albicans and Staphylococcus aureus.

Instrument

Extraction of pigment: Accurately weigh 1 g of mountain blue powder that has been pulverized through a 40 mesh sieve, place it in a 100 mL round bottom flask, add deionized water according to the designed ratio of material to liquid, and place it in computer microwave solid-liquid phase synthesis/extraction. Extract, filter, and volume in the instrument.

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